A facile synthesis of a solvent-dispersible magnetically recoverable Pd-0 catalyst for the C-C coupling reaction

 
Abstract: Solvent-dispersible magnetite particles (Fe3O4) functionalized with dopamine (DA) and N, N-dimethylglycine (DMG) were successfully prepared by a one-pot synthesis method with environment friendly materials. Then Pd-0 nanoparticles were anchored onto the functionalized Fe3O4. The prepared materials were thoroughly characterized by TEM, XRD, XPS, FT-IR and VSM. The resultant magnetically recoverable Pd catalyst exhibited excellent catalytic activity for the C-C coupling reaction. In addition, this catalyst revealed high efficiency and stability during recycling stages. This work should be useful for the development and application of a magnetically recoverable Pd catalyst on the basis of green chemistry principles.

KeyWords Plus: FREE SONOGASHIRA REACTIONS; RESIN-SUPPORTED PD(II); HECK REACTION; ARYL HALIDES; PALLADIUM CATALYST; AEROBIC CONDITIONS; HIGHLY EFFICIENT; SUZUKI REACTIONS; NANOPARTICLES; WATER

Published in RSC ADVANCES, 6 (61):56028-56034; 10.1039/c6ra11674d 2016

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